Effect of the applied amount of sulphur and dolomite on Pb form distribution in yellow-cinnamon soil was investigated by indoor incubation experiment with the sequential extraction method. The results showed that the content of exchangeable Pb trended to increase with a single high sulphur treatment; soil pH value increased when treated with dolomite, which significantly promoted Pb transformed from the exchangeable form to the carbonate bond and the Fe/Mn oxides bond forms, moreover, it was hard to change this trend by either application of a single sulphur element or increasing the applied amount of dolomite in the studied range.